Home Cosmetic Science Talk Formulating Azaleic Acid lotion formula: good or crappy?

  • Azaleic Acid lotion formula: good or crappy?

    Posted by Margaret on April 3, 2024 at 11:27 am

    Would this proposed lotion be a failure with the azaleic acid (AZA) crystallizing after the lotion cools?

    I have looked over various prototype formulae of the azaleic acid producers: some have the AZA added to a heated water phase, some add it when the product is at 40C, some just add each ingredient at room temperature & mix it all together, so I am CLUELESS as to what to actually do for a lotion.

    I do NOT have the ingredients to make a gel, I wish to make a lotion IF it’s possible.

    The 10% AZA is to treat rosacea.

    The AZA would be heated along with the other water phase ingredients to 75-80 Celsius. Oils phase would be heated as well to ensure everything’s dissolved and homogeneous.

    Water Phase:

    68% water (approx)

    8% propylene glycol (I want to avoid the stickiness of glycerin, but I could do 50/50 with PG)

    10% azaleic acid (powder form)

    0.5% allantoin

    0.2% sodium phytate

    0.3% citric acid (50% sol’n) to get to pH 4.5 - 5

    Oils Phase:

    8% shea light ester

    4% polawax emulsifier (cetearyl alcohol & Peg-20 stearate)

    1% dimethicone (350 cs I think)

    0.1% Vitamin E

    0.3 % xanthan gum

    Preservative when at 45 Celsius

    0.5 % Germall

    THANKS FOR ANY INPUT!!!

    • This discussion was modified 4 weeks ago by  Margaret. Reason: spelling error
    Margaret replied 3 weeks, 2 days ago 2 Members · 2 Replies
  • 2 Replies
  • chemicalmatt

    Member
    April 8, 2024 at 12:43 pm

    This is pushing the solubility limit for azelaic acid unless you raise the pH closer to neutral with a metal hydroxide. With a little more Polawax this should work. Xanthan gum will be dispersed into water first (NOT in the oil phase) then add AZA into water at temperature, adjust pH to 5.5 - 6.5, then proceed as planned and see what you get. I would add a little cetyl alcohol to mitigate the “soaping” from the PEG ester and improve stability at same time. Kudos to you for employing Germall as preservative.

  • Margaret

    Member
    April 8, 2024 at 2:59 pm

    Thanks so much Matt!

    I had forgotten to write in the cetyl alcohol in my formula (doh!!). I think I have run out of it, so I’ll use 0.5% brassica alcohol.

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