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  • PhilGeis

    Member
    September 13, 2021 at 10:28 am in reply to: Preservative needed for cleaning product with pH 10?

    Not aware of a “safe use” or “use by” provision for household products, esp. re. micro contamination.  Can you share the regulation?  
    Household product preservation targets manufacturing contamination, not in-use contamination by consumers that is a concern for cosmetics.
       
    Whether appropriate and required for household product or not, use by, ex dates or the moronic PAO should not be used to excuse unstable products.    Why do you think no consumers will not be using your product one year after manufacture?

  • PhilGeis

    Member
    September 9, 2021 at 2:16 pm in reply to: Need Guidance for Liquid dishsoap

    Liquid dish soap is typically alkaline in pH and benzoate alone even at favorable pH by itself is a poor preservative .  These products are typically preserved.
    Consider Benzyl or Methyl isothiazolinone 

  • PhilGeis

    Member
    September 9, 2021 at 1:00 pm in reply to: Preservative needed for cleaning product with pH 10?

    Use by date - on what would you base that and can you say more about “manufacturer guidelines.”

    In what country will you sell?

  • PhilGeis

    Member
    September 7, 2021 at 1:54 pm in reply to: QC for Ingredient
  • PhilGeis

    Member
    September 7, 2021 at 10:17 am in reply to: EDTA

    Chelators are not equal.  Like preservatives, subordinating a functional ingredient to serve a secondary claim is not without risk.  All you have to judge is a PET test too blunt to dissect that risk.  

  • PhilGeis

    Member
    September 6, 2021 at 5:59 pm in reply to: EDTA

    For preservation (booster)  - WITH a preservative.  Those are good preservative systems and EDTA enhances.

  • PhilGeis

    Member
    September 6, 2021 at 1:48 pm in reply to: EDTA

    For preservation - yes.

  • PhilGeis

    Member
    September 6, 2021 at 10:31 am in reply to: Effect of high pH on microbes

    Bacterial spores and spores of many fungi will not be killed.  There isn’t a good answer for speed of kill for other/vegetative cells but you can’t count on complete kill.

  • PhilGeis

    Member
    September 4, 2021 at 10:52 am in reply to: Glyceryl Caprylate (GMCY) vs Glyceryl Caprylate Caprate

    These are really poor “boosters” - esp. vs Gram negatives and their esterases.  

  • PhilGeis

    Member
    September 3, 2021 at 9:45 am in reply to: Preservatives in personal lubricant

    What standard are you using for PET?  Don’t think either USP 51 nor EP has relevant day 7 for what I’d assume is your category.  Doesn’t change the need here for better preservation that might be better served with a paraben.

    Suggest you review what’s used in marketed products - esp. US where I think 501k filling is needed.

  • Gamma irradiation is the best method for clay.    Dry heat 180C for 2-3 hours would theoretically do it - if you get penetration and the material is dry.

    Please don’t use “nasties” - no need for the mommy blog BS.

  • PhilGeis

    Member
    September 2, 2021 at 9:27 am in reply to: Preservative Help - Quickly glance at my conditioner formula?

    zetein said:

    @PhilGeis Can the cationic surfactant in conditioner be relied on for anti-microbial? If yes, what should the concentration and pH be?

    Nope tho some  might have a small effect, none adequately preserve.  Note Downy and others with enough cationic to work through the wash still need preservatives. 

  • PhilGeis

    Member
    September 2, 2021 at 9:25 am in reply to: Sustainable Mica versus Iron Oxide

    Claim is at best mislabeled - they could call it “blessed” with the same accuracy.  More importantly, how is it assured?  Is there a rip off org like EWG that extorts to condifrm?

    Confident that brief UN description took years,  millions of dollars and extensive travel by authors to produce.
    EU, US and major nations generate their own policy and those are largely picked up by smaller nations if they bother, not UN’s.

  • PhilGeis

    Member
    September 1, 2021 at 3:28 pm in reply to: Preservative Help - Quickly glance at my conditioner formula?

    Sorbate is so weak and the others are 100% useless as “preservatives”. This is not hurdle - it’s total BS.

    Maybe they found this passed USP 51 - hardly a recommendation.  One needs to design a system that should work and confirm efficacy with 51.    51 by itself is not a valid test for efficacy.

  • PhilGeis

    Member
    September 1, 2021 at 3:06 pm in reply to: Preservative Help - Quickly glance at my conditioner formula?

    Sorbate alone is not useful and 0.1% is stupid.
    Plastic - polyethylene? flip top or screw off?
    Heat - how high and is it packed out hot/warm?

  • PhilGeis

    Member
    September 1, 2021 at 2:59 pm in reply to: Hydrochloric acid upper safe limit for rinse off product?

    Personal protection equipment for you - eye shields etc.

  • PhilGeis

    Member
    September 1, 2021 at 2:52 pm in reply to: Hydrochloric acid upper safe limit for rinse off product?

    Use PPE

  • PhilGeis

    Member
    September 1, 2021 at 2:51 pm in reply to: Preservative Help - Quickly glance at my conditioner formula?

    Your biggest issue is with Gram negatives. Wish you could use isothiazolinones - failing that phenoxyethanol or benzyl alcohol at ~0.5%.  Don’t see too much purpose in multiple organic acids - DHA has the most favorable pKa but I worry about stability. Think you also need a chelator - EDTA, phytate.
    What kind of process and package?

  • PhilGeis

    Member
    September 1, 2021 at 2:31 pm in reply to: Preservative Help - Quickly glance at my conditioner formula?

    pH ?

  • PhilGeis

    Member
    September 1, 2021 at 11:09 am in reply to: Sustainable Mica versus Iron Oxide

    UN bureaucracy sticks its fingers in everything.

  • PhilGeis

    Member
    September 1, 2021 at 12:15 am in reply to: Preservative needed for cleaning product with pH 10?

    Dilute soap - any heat in prep?  If water is in control and small batches, prob not with effective cleaning and sanitization.
    If preservative needed - try benzoisothiazolinone (e.g. Proxel) or Gylcoserve (DMDM Hydantoin).

  • PhilGeis

    Member
    August 31, 2021 at 8:09 pm in reply to: Sustainable Mica versus Iron Oxide

     
    And unless your putting mica back, it’s nor more sustainable than petroleum production.

    I suppose we can think of this claim as puffery.  As typically used, “sustainable” is j.ust that

  • PhilGeis

    Member
    August 31, 2021 at 4:43 pm in reply to: Can I combine two preservatives?

    You can - but the combination is not great.  Benzyl or phenoxy with benzoate AND a chelator will do well in a shampoo.  But “natural”  

  • PhilGeis

    Member
    August 31, 2021 at 4:40 pm in reply to: Sustainable Mica versus Iron Oxide

    How is mica sustainable?

  • PhilGeis

    Member
    August 31, 2021 at 4:38 pm in reply to: Need help with blending preservatives and boosters

    Phenoxyethanol at 0.5% and Na benzoate at 0.26%.

    Amen to my colleague Abdullah’s comment!

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