Home Cosmetic Science Talk Formulating Hair Wax Crystals In My Home-brewed Oil Based Pomade

  • Wax Crystals In My Home-brewed Oil Based Pomade

    Posted by carp0824 on May 23, 2017 at 6:07 pm

    Hello Gang,

    I am running into an issue with an oil based pomade that I have been working on. No matter what I do, I end up with little wax crystals, balls, grains, gel pebbles (not sure what to call it). 

    Ingredients:

    • Petroleum - 56%
    • Beeswax - 20%
    • Coconut Oil - 10%
    • Castor Oil - 10%
    • Hemp Seed Oil - 4%

    I have heated the beeswax up to 93.3 C. I ensure all solids have melted. I usually keep it on the heat for about 20 minutes. I add the petroleum and coconut oil at this stage as well. I turn the heat off and add in the castor oil and hemp seed oil. Stir and pour into my container at 62.8 C.

    The next day when I scoop it out, I can feel little gel pebbles in the pomade that do melt down when I rub my hands together. Based off of my process and ingredients, can anyone identify what may be causing this?

    There is little information online. The information I have read is all over the place. The only thing I have found that makes was found on this link http://digitalcommons.usu.edu/cgi/viewcontent.cgi?article=6139&context=etd

    Is it possible the oils are causing this?

    Kind regards,

    zaidjeber replied 7 years, 5 months ago 7 Members · 15 Replies
  • 15 Replies
  • belassi

    Member
    May 23, 2017 at 7:39 pm

    Petroleum?? You are adding gasoline to it?

  • carp0824

    Member
    May 23, 2017 at 7:45 pm

    Petroleum jelly (cosmetic grade).

  • belassi

    Member
    May 23, 2017 at 9:26 pm

    If this is your only problem and otherwise you’re happy, I would try replacing the beeswax with other types, eg microcrystalline. There are many people here who can help.

  • Bill_Toge

    Member
    May 23, 2017 at 9:33 pm

    what grade of coconut oil are you using - is it whole or refined?

    (also, petroleum jelly is called “petrolatum”)

  • DRBOB@VERDIENT.BIZ

    Member
    May 23, 2017 at 11:14 pm

    Beeswax particularly at the level you are using will give crystallization problems: try carnubba which should provide nice properties in the presence of that much petrolatum.

  • carp0824

    Member
    May 24, 2017 at 2:24 pm

    Thank you all for the feedback. It is truly appreciated and valued. 

    @Bill_Toge, the coconut oil is virgin. I initially thought that was the problem so I tried a sample without using coconut oil and obtained the same result.

    @Belassi, I would like to keep playing with the consistency of the pomade. I like the hold that beeswax offers. Maybe I can find a balance between combining the two. 

    @DRBOB@VERDIENT.BIZ, would you say the level of beeswax I’m using is too high or low? Would reducing the amount of petrolatum help? I have noticed that the pomade is on the more oily side of things. I’d like to reduce that aspect. 

  • beautynerd

    Member
    May 24, 2017 at 2:43 pm

    Isn’t cera bellina meant to help in situations like this?

  • carp0824

    Member
    May 24, 2017 at 4:46 pm

    @EliseCortes, I’m not sure as I’m not 100% positive as to what is causing my issue. I’d like to determine the root cause and see if there is a way to adjust my process rather than add another ingredient to the formula. However, if this is the best option then I will investigate.

  • DRBOB@VERDIENT.BIZ

    Member
    May 24, 2017 at 10:22 pm

    Elise problem is crystallization of too much B wax so I would cut it to 10 percent and lower petrolatum to 40 and replace with jojoba to improve oily aestheticsYou can back add paraffin or carnubba if needed to replace B wax

  • zaidjeber

    Member
    May 25, 2017 at 1:33 am

    @carp0824 I did formulate balm with bees wax before and I had the same crystallization problem. I agree with @DRBOB@VERDIENT.BIZ reduce the bees wax and try to replace with carnubba, paraffin, HCO or a mixture of all three. BTW ain’t you using any preservatives in your pomade?!   

  • carp0824

    Member
    May 25, 2017 at 2:40 pm

    @DRBOB@VERDIENT.BIZ, I’ll give this a shot. Thank you for the advice.

  • carp0824

    Member
    May 25, 2017 at 2:42 pm

    @zaidjeber, I wouldn’t think a preservative would be needed in an oil base due to there not being any water present in the formulation. 

  • OldPerry

    Member
    May 25, 2017 at 6:37 pm

    @carp0824 - If you want to find the root cause, do a knockout experiment.

  • carp0824

    Member
    May 26, 2017 at 2:34 pm

    @Perry, I just started doing this yesterday. So far I have one ingredient left to remove and haven’t experienced any change in the results yet. Thank you for the recommendation. 

  • zaidjeber

    Member
    May 29, 2017 at 1:00 am

    @carp0824 you are right, my point is “better safe than sorry”  

Log in to reply.

Chemists Corner