Home Cosmetic Science Talk Formulating Scalp serum (O/W emulsion) FAIL! PLEASE HELP!

  • Scalp serum (O/W emulsion) FAIL! PLEASE HELP!

    Posted by arastellar09 on January 16, 2025 at 5:54 am

    Phase A:

    Distilled water (80%)

    Herbal extract (5%) {extracted by 70% ethanol}

    Phase B:

    Wanult oil (1%)

    Rose geranium E.O. (0.6%)

    Tocopherol mixed (0.4%)

    Symbiosolv Clear + (5%)

    Phase C:

    Sodium Ascorbyl phosphate (2%)

    Niacinamide B3 (1.2%)

    Pyridoxin HCl B6 (0.3%)

    D Biotin B7 (0.5%)

    Phase D:

    Clear Xanthan gum (0.5%)

    Acacia gum (0.5%)

    Propanediol (2%)

    Preservative:

    Optiphen + (1%)

    PROCEDURE:

    1) Mix Phase A and Phase B thoroughly in two separate breakers, then combine to make the O/W emulsion.

    2) Check the pH of the emulsion, should be around 6-6.5 for the vitamins to be effective. Add Phase C and stir. Check and adjust pH again to around 6.5.

    3) Mix all the ingredients of Phase D together and gently add it to the emulsion to thicken it.

    4) Later, add the preservative.

    PROBLEM:

    1) After few days for keeping the emulsion undisturbed, I can notice the oil droplets floating on the surface of the emulsion.

    2) There is a darker slimy thing settled at the bottom of the beaker. I don’t know what it is?

    Can anyone help? what went wrong?

    arastellar09 replied 5 hours, 10 minutes ago 1 Member · 0 Replies
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