Home Cosmetic Science Talk Formulating Water-Based Lubricant - Formula Validation

  • Water-Based Lubricant - Formula Validation

    Posted by Cosmetic_Chemist on June 27, 2022 at 8:51 pm

    Hi everyone!

    I was hoping someone could validate my formula - mainly I want to know if the preservative system is okay

    water - Qs
    Hydroxyethylcellulose - 1.0%
    Propanediol - 3%
    Sodium Benzoate - 1.0 
    Potassium Sorbate - 0.5%

    any other ingredients that you think I should add?
    It has to be clean at sephora! 

    Thank you!

    Cosmetic_Chemist replied 2 years, 4 months ago 9 Members · 19 Replies
  • 19 Replies
  • Graillotion

    Member
    June 27, 2022 at 9:03 pm

    That question cannot be answered…without knowing the pH (as your system is pH dependent.) 

  • MarkBroussard

    Member
    June 27, 2022 at 9:55 pm

    Hi everyone!

    I was hoping someone could validate my formula - mainly I want to know if the preservative system is okay

    water - Qs
    Hydroxyethylcellulose - 1.0%
    Propanediol - 3%
    Sodium Benzoate - 1.0 
    Potassium Sorbate - 0.5%

    any other ingredients that you think I should add?
    It has to be clean at sephora! 

    Thank you!

    @Cosmetic_Chemist

    Firs of all you are too high on both Sodium Benzoate and Postassium Sorbate.  That should be more in the range 0.4% and 0.2%, respectively.

    Second, your pH is going to have to be less than 6.0 and more preferrably around 4.5

  • rodb1958

    Member
    June 28, 2022 at 2:42 am

    while agreeing with the above re content and pH the only real way is to send your product out for a preservative challenge test.

  • ketchito

    Member
    June 28, 2022 at 12:05 pm

    @Cosmetic_Chemist Not sure that system would be enough to protect against all groups of microorganisms, with so much available water in your system, good amount of HEC and Propanediol (nutrients), lack of surfactants (they work in synergy with organic acids) and lack of boosters (like chelators). Not to mention the required low pH.

  • MarkBroussard

    Member
    June 28, 2022 at 12:50 pm

    @Cosmetic_Chemist

    Generally, no your preservation system is weak.

    You should add a chelator, Sodium Benzoate and Potassium Sorbate both work by the same mechanism of action … use only one, not both and preferrably Sodium Benzoate.  You’ll need to add an anti-bacterial and a pH adjuster.

  • Cosmetic_Chemist

    Member
    June 28, 2022 at 7:27 pm

    pH will be 4-5 

    pH will be adjusted with citric acid. I will also be adding Sodium Phytate as a cheleter/booster. 

    @MarkBroussard
     Which antibacterial do you recommend instead of potassium sorbate?

  • MarkBroussard

    Member
    June 28, 2022 at 10:21 pm

    @Cosmetic_Chemist

    Do you have any restrictions on what you can use?

  • Cosmetic_Chemist

    Member
    June 29, 2022 at 12:10 am

    It just needs to be clean at Sephora

  • Squinny

    Member
    June 29, 2022 at 2:53 am

    I’d be concerned to make sure it isnt going to cause yeast infections ( I assume it is for the down under area?) 

  • Abdullah

    Member
    June 29, 2022 at 5:15 am

    What is this used for?

  • Cosmetic_Chemist

    Member
    June 29, 2022 at 1:21 pm

    It is an adult novelty product and will be used down under. 

    Would this current formula likely cause a yeast infection?

    If i use Phenoxyethanol and EDTA instead of current preservatives, would I get a better result?

  • MarkBroussard

    Member
    June 29, 2022 at 2:34 pm

    Your best bet would be Sodium Benzoate, Phenoxyethanol, EDTA … Yes, that would pass Clean at Sephora standards

  • Abdullah

    Member
    June 29, 2022 at 2:49 pm

    Is it for personal use or for selling? 

    I would suggest increase Propanediol to ≥10% for water activity, pH 4 and a blend of phenoxyethanol & parabens. 
    I am not sure about compatibility of phenoxyethanol with 1% HEC though. @PhilGeis may have better suggestions.

    That is the most gentle part of body and those preservatives are not so gentle.

  • MarkBroussard

    Member
    June 29, 2022 at 4:24 pm

    Parabens are not allowed under Sephora Clean requirements

  • Cosmetic_Chemist

    Member
    June 29, 2022 at 5:21 pm

    water - Qs
    Hydroxyethylcellulose - 0.75%
    Propanediol - 5%
    Glycerin - 3%
    Sodium Benzoate - 0.4%
    Phenoxyethanol - 0.3%
    EDTA - 0.1%
    Aloe Vera Juice - 0.05%

    Would this be a better formula? 

  • jcast

    Member
    July 1, 2022 at 4:14 pm

    I have made a nice lubricant with Natrosol 250 HHR (HEC) at 1.25%, propanediol, other humectants and Phenoxyethanol and Ethylhexylglycerin 90:10, respectively.

  • PhilGeis

    Member
    July 4, 2022 at 4:53 pm

    water - Qs
    Hydroxyethylcellulose - 0.75%
    Propanediol - 5%
    Glycerin - 3%
    Sodium Benzoate - 0.4%
    Phenoxyethanol - 0.3%
    EDTA - 0.1%
    Aloe Vera Juice - 0.05%

    Would this be a better formula? 

    Looks ok - maybe phenoxy at 0.5% and Na benozate a bit less maybe 0.26%.
    Will you challenge test through stability per ISO?
    Do watch out for contaminated aloe juice.

  • MarkBroussard

    Member
    July 4, 2022 at 5:16 pm

    water - Qs
    Hydroxyethylcellulose - 0.75%
    Propanediol - 5%
    Glycerin - 3%
    Sodium Benzoate - 0.4%
    Phenoxyethanol - 0.3%
    EDTA - 0.1%
    Aloe Vera Juice - 0.05%

    Would this be a better formula? 

    @Cosmetic_Chemist

    I would replace Glycerin with Pentylene Glycol.  Glycerin @ 3% is going to be a sticky mess and most women don’t like Glycerin in products for intimate areas.  I would also eliminate the Aloe Vera Juice … It’s really not doing anything for your formula.  Follow Phil’s recommendations on your preservative percentages.

    This will probably fall under a 510K Medical Device.  The required testing is expensive … on the order of $200K.

  • Cosmetic_Chemist

    Member
    July 4, 2022 at 6:45 pm

    Thank you so much! I am going to try out the new version and will report results once I hear back from the client! 

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